How To Set Up A Science Lab Report
The Laboratory Report1,2
Authors: One thousand. C. Nagan and J. Yard. McCormick
Introduction
The research paper is the primary means of advice in scientific discipline. The research paper presents the results of the experiment and interpretation of the data, describes the rationale and design of the experiment, provides a context for the results in terms of previous findings and assesses the overall success of the experiment(s). Scientists working in industrial laboratories exercise not write as many journal articles as their colleagues in academia, simply they routinely write progress reports, which take the same class as a journal article. So no affair what your career goals are, it is of import that you get familiar with this style of writing.
There are set up rules for preparing a periodical article (or a laboratory study). The style requirements vary only slightly from journal to periodical, just there are far more similarities than differences in the scientific writing manner. If y'all are writing an article for publication in a particular journal (or preparing a laboratory report in the style of a particular journal) you should consult the Instructions to Authors section of the journal'south website (this information is also included in the periodical'south first issue of each twelvemonth).
There are several style guidesthree, 4 and manufacturesv to help scientists and students prepare their manuscripts. The most useful of these to chemists is the American Chemic Society'due south (ACS) ACS Style Guide, which may be establish in the Truman library or may be purchased from the ACS web site. Considering of the variation in periodical styles, and the requirements for a specific grade, your teacher will inform you lot of specific style requirements for his or her class. This guide is based on the Journal of the American Chemical Society way,6 and is meant to provide a proficient starting point for writing a laboratory report. It is not meant to be the definitive fashion guide; y'all must arrange your style to your audience and the periodical in which your results volition be published.
General Editorial Issues
Although we shouldn't, all of u.s.a. are swayed by first impressions. How your newspaper appears to the journal editor or reviewer is their start impression of your scientific discipline, and it will color their impression of your results, if you let it. Nada is worse than a sloppily prepared paper with no page numbers, a font that tin can't be read or which is full of grammatical errors. Recollect that everyone will presume that if you did not accept the time to write your paper carefully, you did not have the time to do your science carefully.
The post-obit are some full general editorial guidelines to follow that will leave a expert first impression with your readers.
- 1) Double-space your newspaper throughout (including figure captions and tables, too).
- 2) Use a reasonably sized font such equally 12 point Times.
- three) For figures, you may cull to utilise a sans-serif font for better graphics quality such as Arial or Helvetica.
- 4) Utilise at to the lowest degree 1" margins on all sides.
- 5) Number the pages. Identify the page numbers in the top, right-mitt corner, or centered on the lesser of the page. Either style is acceptable and whichever one you choose remain consistent in your numbering scheme throughout the paper.
- 6) Practise not first sentences with symbols or numbers; rather, spell out the full name of the symbol if information technology is used at the offset of the sentence. For example, write "Alpha-lactalbumin" instead of "α-Lactalbumin" when outset a judgement. Too spell out symbols or numbers in a championship, except when part of a chemical proper name (e.g. 2-hexanol).
- 7) Spell check the document thoroughly. Accept someone, who volition give you an honest and complete critique of your newspaper, read the paper. Revise, revise, revise!
Full general Stylistic Issues
Uniformity of style is the primal to scientific communication. The journal editors, the referees who review a manuscript, and the journal readers who are interested in the results presented in a paper all await sure things to be present in a manuscript and that they are in a certain order. Just similar the sloppy-looking paper, a paper that does not adhere to the expected fashion reflects poorly on the author, no affair how skilful the science is.
- 1) The paper should be written in a third person, passive vocalism. Occasionally, merely rarely, it is appropriate to utilize "we" when describing the intention of the authors. Information technology generally depends upon the intended field of study of the sentence. Consider the two sentences below:
- a) Calcium solid (v g) was poured into a beaker.
- b) Nosotros poured calcium solid (5 g) into a chalice.
- In the first judgement (a), which is passive, the field of study is the calcium solid. In the 2nd sentence, the subject is the experimenters. In scientific manufactures, the bailiwick is most often the scientific discipline and not the experimenters.
- 2) Use the past tense in general (e. g., what was or has been done). However, use nowadays tense when describing properties of molecules or organisms because they nonetheless take these properties.
- iii) Unless directed otherwise, assume the reader of your laboratory report is your peer, the average chemical science educatee, non the chemistry professor. Therefore, everything should be explained equally if the reader knows some chemistry, simply is not an expert in the bailiwick of the paper. Past no means does the reader know what you are doing, or why yous are conducting your experiment. Recollect near what you would want to know about the subject if yous were the reader.
- four) Avoid repetition in language. Endeavor not to start each judgement with the same construction and words.
- five) Do not apply quotes. Unlike humanities or literature papers, quotations are rarely plant in scientific articles. Still, it is appropriate to paraphrase other authors.
- 6) Explicate technical terms.
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- Example
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- "Hemoglobin has a Colina constant, a value that describes the degree of cooperative ligand binding, of 2.eight."
- 7) Ascertain abbreviations.
-
- Instance
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- "The official colors of Truman State University (TSU) are majestic and white."
- eight) Identify a space between a number and a unit of measurement.
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- Instance
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- "Sephadex (x g) was combined with deionized HtwoO (100 mL) at 25 °C."
- ix) Exercise not outset a judgement with a number or "Effigy ane" or "Table 1", etc..
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- Correct: Milk samples (50 μL) were analyzed past high operation liquid chromatography nether three unlike buffer conditions (Figure 1).
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- Incorrect: Figure 1 shows the loftier performance liquid chromatography chromatograms for the sample run under three different buffer conditions.
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- Incorrect: fifty μL of milk was analyzed by loftier performance liquid chromatography using three dissimilar buffer conditions.
- 10) There are three ways to refer to a newspaper in the text.
- For example, the citation of the work authored past Jackson, A. M.; Wilson, R. S.; Houk, K. L.*, could appear in the text in whatsoever of the post-obit means. (Notation that et al. is an abridgement for et alia and that it is italicized because it is not English.vii)
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- a) Jackson et al.
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- b) Jackson and coworkers
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- c) Houk and coworkers
In the final case we assumed that the author whose name is starred is the principle investigator on the project, and gave them more than credit for the work. Note that it is an American convention to list the principle investigators last, while many European and Japanese journals place them first.
- Often there are 2 principle investigators, and in this case both should be mentioned. For example, the piece of work by Jackson, A. M.; Wilson, R. S.*; Houk, K. L.* should be referred to, in the format given in example (c) in a higher place, as "Wilson, Houk and coworkers". If there are more than than two principle investigators, it is all-time to employ either of the formats given in instance (a) or (b), or to use some other wording to avoid this construction entirely.
Organisation/Components
Sections
Sections should announced in your paper in the lodge described beneath. All sections but the title have the department explicitly labeled, usually in assuming letters to differentiate it from the residuum of the text, and left aligned on the page. A blank line should appear after the last word of the section to split up the various sections, but a line should not be placed after the section title.
- 1) Championship/Championship page
- 2) Abstract
- 3) Introduction
- 4) Experimental (Materials and Methods in some journals)
- 5) Results
- 6) Discussion
- 7) Conclusions
- 8) Acknowledgements
- nine) References
- 10) Tables
- 11) Schemes
- 12) Figure Legends
- xiii) Figures
- fourteen) Supporting Information
Please note that you should not physically gather your newspaper in this club. Instead, it is suggested that you compose: a) Materials and Methods, b) Figures, Figure Legends and Tables, c) Results, d) Discussion, east) Conclusions, f) Introduction and Schemes, g) Abstract, and h) Title. So put all the sections together in the final paper in the order outlined above.
A template is bachelor to assistance you organize your report. Click here to larn more than about it.
Subsections
It may be helpful to organize sections farther into subsections. These subsections should accept their own titles that are italicized and followed by a period.
Description of Paper Components
Title/Title Page
A title reflects the emphasis and contents of the paper. Information technology tells the reader the newspaper's topic and it too entices the reader to continue reading further. Therefore, it is not uncommon for the title to reveal the results or major conclusions of the experiment. Examples are given below. The title should be on its own page (the title folio), left-aligned at the acme of the folio, in bold letters. Note that in some journals the title's font size is 2 points larger than the text (i. e., 14-betoken, if the remainder of the newspaper is in a standard 12-point font). Still, this is not standardized and you should check with your teacher for which format he/she wants you to follow.
The title must be brief (ii lines maximum) and grammatically correct. Under the title, write your name and your professional accost in italics (Section of Chemistry, Truman Land University, 100 East Normal, Kirksville, MO 63501).
- Example Titles
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- ane) Conclusion of the Differential Fluidity of Water and Benzene by Viscosity Measurements
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- 2) Purification of Alpha-Lactalbumin from Bovine Skim Milk by Immobilized Metallic Ion Affinity Chromatography
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- 3) Synthesis and Characterization of Potassium Tris(oxalato)ferrate(III)
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- 4) Ionic Composition of Drinking H2o Influenced by Pipe Materials: An Atomic Absorption Spectroscopic Analysis
Abstract
The abstruse is a one-paragraph summary of the newspaper that is written in the nowadays tense. As the abstruse is the only office of the paper that is entered into article databases, it should exist able to stand alone, separate from the paper. The commencement one to 3 sentences of the abstract should briefly introduce the reader to the problem studied. Side by side, the scientific approach, major results and primary significance of the findings should be presented. The abstract is by and large 150-200 words (less for shorter papers). This section is normally written after the body of the paper. Because the abstract is separate from the paper, all abbreviations should exist written out, or defined, and any references should be written out in full. An example of how a reference might appear in an abstruse is
- Inhaled fumes from permanent markers take been shown to cause encephalon damage (Johnson, A. J. Permanent markers and the brain. J. Am. Brain. Res. 2004, eighteen, 215–218).
Note that in some journals that inclusion of the title in a reference is not required (vide infra).
Introduction
The introduction should present the scientific problem at hand to the reader. Explicate to the reader why the experiment was conducted, how information technology was designed and perhaps, if appropriate, what was found. Literature that is relevant should be incorporated and will assistance the reader sympathize the context of your study. A good rule of thumb is to first at the almost general topic and progressively move towards the specific. Hither is a general outline for an introduction:
- I. Broad significance of the topic to the chemistry discipline and society in general
- II. Introduction to the topic within chemical science
- III. Clarification of the specific problem
- Four. General goals and significance of the experiment or inquiry topic
In this department, consider including figures, schemes and equations that complement the text.
While this is like to the information that y'all should have written your notebook, the introduction to a paper is different than the background that you included for an experiment (or experiments) in your notebook. Recollect that you are trying to reach a larger, more general audience with your paper, and the introduction must be structured to describe the reader in and help them focus on your important results.
Experimental
The experimental section of your paper should be a logical, coherent recount of the experiment(s) conducted. This section should be complete enough for a trained scientist to pick up your study and replicate your experiment. The experimental section in a laboratory report is more concise than the corresponding section in the laboratory notebook. It should not be a step-past-footstep process of the activities carried out during the laboratory menstruum.
The first paragraph of the experimental section contains information on cardinal chemicals used in the procedure. When the chemicals are used as received, there will normally be a statement to that effect and further details are not usually necessary. You will list the chemic supplier's name and the substance's purity will be noted in cases where the chemical is hard to observe, it is of a special purity or if there is only one supplier. Do not listing lot numbers. If a starting material was synthesized according to a literature process, then state this in the opening paragraph and reference the process. If purification or drying of the compounds is required, information technology is described hither, as well.
The first paragraph frequently will also list the instruments used to characterize the newly synthesized substances. All instruments and equipment should be specified including the model number of the musical instrument and the name of the manufacturer (serial numbers are non included). When a spectroscopic or physical method is the focus of the study, information technology will be described in its own subsection. You are not required to write the experimental in this fashion.
For common techniques, laboratory textbooks should be referenced. However, if a previously published procedure was modified, then this is stated and simply the modifications performed are included. If the procedure is your own, then outline the procedure with the main points, including details that are critical to replicating the experiment. These might include the type and size of your HPLC column, the buffer or the concentrations of chemicals.
When the syntheses of substances are reported, the synthetic procedure used to make each substance is described in its own split paragraph. The paragraph begins with the name of substance, or its abbreviation (if the abridgement was defined earlier in the paper), in bold face. If numbers are assigned to the compounds, these are likewise included (in parentheses). Often the synthesis will exist written out, even when a literature procedure was followed. The mass and percent yields must be reported. Some of the new chemical compound'south characteristics are included at the stop of the paragraph describing its synthesis. These include: melting betoken range (and literature value, if known), elemental analysis (both calculated and found), selected peaks from the mass spectrum (with assignments), selected IR peaks (also with assignments), and any NMR peaks with their chemic shift, multiplicity and integration (you will often find the observed coupling quoted and the assignment of the peaks). The following is an example of how to report a compound'south synthesis.
- Tris-(2-pyridylmethyl)amine: To a stirred solution containing 10.11 g 2-pyridylmethyl chloride hydrochloride and 3.20 ml 2-pyridylmethyl amine in 20 ml HiiO was added in a wearisome, drop-wise way (~1 driblet every 25 sec) a solution containing 5.03 g NaOH in 12 ml HiiO and so that all of the solution was added in about one.v hr. Upon complete addition of the NaOH, the reaction mixture was heated on a heating drape to 70 ºC for 20 min. The cooled reaction mixture was and then extracted four times with 50 ml CH2Cltwo. The combined extracts were dried over Na2SOiv and the CH2Cl2 was removed using a rotary evaporator. The resulting carmine oil solidified upon standing. The cherry-red solid was and then dissolved in a minimum of hot hexane. The yellow solution was decanted from a ruddy oil which did not dissolve and filtered hot. Upon cooling the product crystallizes in large needles, which were recovered by filtration and air-dried. Recrystallization from hexane gave 2.08 thousand of the product (23% yield). The melting betoken of product is 85 ºC, precipitous (literature 87 – 89 ºC).ref oneH NMR (CDClthree, ppm): iii.89 (s, 6 H, methylene), 7.14 (m, J = 1.3, half dozen.1 Hz, 3 H, pyridyl), vii.58 (d, J = 7.8 Hz, three H, pyridyl), 7.63 (thou, J = 1.8, 7.6 Hz, 3 H, pyridyl), 8.15 (thousand, J = 0.9, 4.nine Hz, six H, pyridyl). 13C NMR (CDClthree, ppm): 60.13 (methylene), 122.01, 122.97, 136.48, 149.06, 159.25 (pyridyl).
The experimental department has two quirky wrinkles on the full general scientific manner. These are:
- 1) when citing previously published procedures, authors' names are more often than not not included,
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- Correct "Purification of the bovine brain isolate was performed co-ordinate to previously published procedures.ref "
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- Incorrect "The previously published process of Jackson et al. ref was followed with modifications outlined below."
- 2) when citing the utilize of a kit, pre-packaged-assay or other commercial equipment with directions, include just the company's name in parentheses; it should non exist a total reference.
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- Example
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- "The Bradford assay (Sigma) was carried out to determine the total poly peptide concentration of the five protein isolates.
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Results
In the Results section, the results are presented and summarized in a reader-friendly form. Raw data are not presented here. For instance, it is appropriate to include the average calculated concentration of a solution simply not the original absorbance values that were collected from the spectrophotometer; that data is best left in your laboratory notebook.
Graphs and tables oftentimes brand the information easier to interpret and more understandable (click hither to review graph preparation). A graph is presented in the paper as a effigy. In general, a graph or table is an advisable representation of the data when more than than ii or 3 numbers are presented. Data that are presented in the form of a graph or table should be referred to but should not be repeated verbatim in the text as this defeats the purpose of a graph. More data on figures and tables is presented afterward.
The Results section also reports comparable literature values for the properties obtained and/or calculated in the paper. Observation of trends in the numerical data is acceptable. However, interpretation of the trend should be saved for the Discussion section.
Think, do not simply report your numerical results. The Results section must have a narrative that describes your results. This narrative can include a description of the data (such every bit spectra or information in graphs), what issues were encountered during data conquering (and how they were resolved, or not) and a full general description of how the raw data were candy to give the final results (not a footstep-by-footstep description of everything you did). The reader wants to know what y'all did, how yous did it, what bug you encountered and finally what your results were. Each of these topics must be addressed in the Results department in a way that is articulate, withal concise.
Word
This is the department where the results are interpreted. This section of the paper is coordinating to a contend. Y'all need to nowadays your data, convince the reader of your data's reliability and nowadays bear witness for your convictions. Offset, evaluate your information. Do yous have adept, mediocre, terrible, or united nations-interpretable data? Evaluate your results by comparison to literature values or other precedents. Explain what results should take been obtained and whether you obtained these expected values. Note that even if expected results were not obtained, you did not fail. Unexpected results are often the most interesting. Mayhap your hypothesis was not right. Why is this? What new hypothesis practice your data propose? If you feel that your results are non reliable, y'all need to explicate why. Employ statistical assay or chemical principles to support your claims. Was there a systematic mistake? Is the mistake due to the limitations of your appliance? Does your data look the aforementioned to inside a standard divergence? Evaluate the statistical significance of your data (click hither to review the statistical treatment of data). After validating your data, yous should interpret your results; state what you believe your results mean. How practise your results help united states of america sympathise the scientific problem? What practice your results mean in the context of the bigger picture of chemistry, or of scientific discipline? How do your results chronicle to the concepts outlined in the introduction? Do not assume that your experiment failed or was successful. You need to prove to the reader, with logical arguments and supporting testify, the value of your study.
The conclusions that you lot wrote in your laboratory notebook are a good starting bespeak from which to organize your thoughts. Your paper'southward give-and-take section is structured very similarly to the conclusions department in your notebook, and information technology might exist good idea to review that now (click here to review the structure of the conclusions in the laboratory notebook).
Conclusions
The Conclusions section is typically a one-paragraph summary of your laboratory report. Hither you summarize the goal(s) of your experiment, land whether you reached that goal, and draw briefly the implications of your study. Note that in some chemistry sub-disciplines information technology is adequate to combine the Give-and-take and Conclusions sections. Consult your grade syllabus or check with your instructor on the specific format to exist used in your class.
Acknowledgements
The Acknowledgements section is where you lot give thanks anyone who helped you significantly with the projection or with the manuscript. For example, you would thank your laboratory partners if they're non authors on the paper, anyone who helped with the design of the experiment or the preparation of the paper. You might too include funding sources such as a Truman State University summer scholarship or a National Institutes of Health grant.
References
Most of the ideas presented in your paper are probably not exclusively yours. Therefore, you should cite other people's piece of work wherever appropriate. However, yous practice not demand to cite information that is common knowledge or is exclusively your idea. The References department is a compilation of all citations fabricated within the paper. It is not a bibliography and therefore should not listing sources that are not straight referred to in the text.
References Format
The format of references varies amongst journals. For your chemistry laboratory reports, you should follow, by default, the ACS guidelines as outlined in The ACS Style Guide and Journal of the American Chemic Social club, JACS (all examples given in this handout suit to JACS format). If your professor requires you to conform to a specific journal's format, wait at articles from that journal or refer to the journal'south "Instructions to Authors." The specifications for nigh ACS journals are:
- one) References should be compiled at the end of the paper in the References section.
- 2) References should be numbered in the order that they appear in the paper. For citations in the narrative, numbers should be superscripted and appear after the punctuation marker.
- y lines should exist inserted between reference entries.
- 4) This department should be double spaced just like the remainder of your newspaper.
- 5) A reference is only listed in one case in the References section. If multiple citations of the reference are fabricated in the text, then the number respective to that reference is placed in the text each fourth dimension. The common abbreviations used in footnotes and references (due east. g., op. cit., ibid.) are non generally used in scientific writing.
Types of References
Manufactures. Journal manufactures are the master source found in laboratory reports. An case is given below. Observe that the authors' initials are given instead of the beginning and middle names. Also, there is no "and" before the terminal writer's proper noun. Some journals require that the article's title exist included in the reference (bank check with your teacher to run into if he/she wants you to use this style). When included, the commodity'south championship should get-go with a capital letter alphabetic character merely the other words in the title, unless they are proper nouns, should non exist capitalized (see below). The periodical title is abbreviated (click here for a list of the ACS abbreviations for common journals). Also, the yr and the comma after the twelvemonth are in bold. Lastly, the reference has inclusive pagination (first and concluding pages are given)
The following are examples of the aforementioned journal commodity with the first given in style where the commodity's title is included in the reference, while the second is in the style where the article'due south title is omitted.
- (one) Bergmann, U.; Glatzel, P.; deGroot, F.; Cramer, S. P. High resolution One thousand capture X-Ray fluorescence spectroscopy: a new tool for chemical characterization. J. Am. Chem. Soc. 1999, 121, 4926-4927.
- (1) Bergmann, U.; Glatzel, P.; deGroot, F.; Cramer, South. P. J. Am. Chem. Soc. 1999, 121, 4926-4927.
Books. Books should be cited in the following manner:
- (2) Brünger, A. T. 10-PLOR Manual, Version 3.1: A System for X-ray Crystallography and NMR; Yale University: New Oasis, CT, 1990; pp 187-206.
- (3) Cheatham, T. E., Three; Kollman, P. A. In Construction, Movement, Interaction, and Expression of Biological Macromolecules; Sarma, R. H. and Sarma, Grand. H., Eds, Adenine: New York, 1998; p. 99.
Estimator Programs. Citations for computer programs vary. If a person in academia wrote the program, there is often a journal-article source. In other cases, the plan is but distributed by a company.
- Periodical Commodity
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- (4) Humphrey, West.; Dalke, A.; Schulten, Chiliad. VMD: Visual Molecular Dynamics. J. Mol. Graph. 1996, fourteen, 33-38.
- Visitor Distribution
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- (5) Case, D. A.; Pearlman, D. A.; Cladwell, J. West.; Cheatham, T. Eastward.; Ross, W. S.; Simmerling, C. L.; Darden, T. A.; Merz, M. M.; Stanton, R. V.; Cheng, A. L.; Vincent, J. J.; Crowley, M.; Ferguson, D. M.; Radmer, R. J.; Seibel, G. Fifty.; Singh, U. C.; Weiner, P. K.; Kollman, P. A. Amber version 5.0; University of California: San Francisco, 1997.
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- (half-dozen) Insight II; San Diego, CA: Molecular Simulations, 2000.
Websites. Journal articles are much preferred over websites. Websites are dynamic and are usually not peer reviewed. One of the only instances when a website is an acceptable reference is when it is referring to a database (still, an article is usually associated with the creation of the database). If you must apply a website, the reference should include a title for the site, the writer(south), year of concluding update and URL. It is unacceptable to use a website as a reference for scientific data or explanations of chemical processes.
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- (seven) Cheatham, T. E., III Simulation Protocol for Polynucleotides; 1998, http://www.amber.ucsf.edu/bister/tutorial/polyA–polyT.
Tables, Schemes and Figures
Tables, schemes and figures are all concise means to convey your message. As yous gear up these items for your report, remember to call up of your reader. Yous want them to derive the maximum amount of data with the minimum amount of piece of work. Pretend to be the reader and ask yourself, "Does this enhance my understanding?", "Tin can I observe everything?", "Can I read it without being distracted?" Poorly prepared tables, schemes and figures will reflect badly on your science, and y'all as a scientist, so think carefully about these items as you set up your report.
Tables
A table is a way to summarize data or ideas in a coherent, filigree-like mode. This is not simply output from a spreadsheet! You should prepare the table in a word-processor so that its formatting matches the rest of your study. In full general, tables have no more than ten rows and columns to avoid overwhelming the reader. One common exception is in review articles (such as in Chemic Reviews) where an author is attempting to summarize results from an entire field. Another mutual exception is in the reporting of 10-ray crystallography data. These tables have their ain special formatting rules, and will not be discussed here.
Tables are referred to in the text equally "Table #". Tables, schemes and figures are labeled separately, with Standard arabic numbers, in the order they are referred to in the paper. Tables accept a table caption, which in some journals appears higher up the tabular array, while in others it appears below. In either case, the table caption is always on the same page every bit the table.
Don't use lines or boxes in your table except where absolutely necessary. Use spaces between your columns instead (helpful hint: information technology is improve to use your give-and-take processor'due south tabular array formatting tools than trying to get the columns to line upwardly using tabs or spaces). All column or row headings should accept clear subtitles and units if needed (usually in parentheses). Whatever numbers that are presented should have proper meaning figures, and an indication of the error should be shown (click hither to review how to written report uncertainty in one's data). An example table is given below.
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- Table one. Aminoacylation efficiency of duplexAla substrates containing base pair substitutions at the 2:71 position.
2:71 Base of operations Pair | gtrue cat/KThou (relative)a | Fold decreaseb | -ΔΔG‡ (kcal/mol)c |
---|---|---|---|
G:C (wild-type) | 1 | 0 | |
Watson-Crick Pur:Pyr Base of operations Pairs | |||
I:C | 0.51 | 1.9 | 0.39 |
Chiliad:4HC | 0.25 | 3.nine | 0.81 |
2AA:U | 0.23 | 4.three | 0.86 |
2AP:U | 0.eighteen | v.6 | 1.0 |
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- aValues reported are averages of at least three determinations with average standard deviations of ±26%.
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- bFold decrease in ktrue cat/KM is given relative to wild-type duplexAla.
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- cΔΔG‡ is defined equally RTln[(kcat/ChiliadChiliad)variant/(one thousandtrue cat/1000M)wild-type], where R=one.98272 cal/mol•K and T=298 K.
Schemes
A scheme is usually a sequence of two or more chemical reactions that together summarize a synthesis. A scheme may besides show the steps in a purification with each footstep or reaction giving the reactants, products, catalysts, and yields. A scheme that shows a chemical reaction may as well show possible intermediates. Note that mechanisms are not usually conveyed using a scheme considering they are more complicated and illustrate where electrons are proposed to move. Mechanisms are most ofttimes placed in a effigy.
It is a common convention in a scheme to write a bold number underneath chemic species referred to in the text. Note that for the first occurrence of the bold number in the text, the chemic'due south proper name is given, merely after that only the bold number is used to identify information technology. This method of defining abbreviations for compounds can besides be done in the experimental section, if there is no scheme. This is very useful when a compound'southward proper name is long or complicated.
The one-step yield is commonly written to the right of the equation, although it is too proper to write the yield under the arrow. Note besides how the reaction conditions can be summarized (i. e., the starting time step below), which saves the reader from flipping to the experimental section for these details.
Each scheme as well has a caption, which is included nether the scheme. The caption should briefly summarize what is in the scheme. If the scheme is from another source, the reference to this source should appear at the end of the caption.
The following is an example of a scheme that might appear in a synthetic paper. The text below it shows how the scheme could be referred to in the body of the paper.
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- Scheme i. Synthesis of benzoyl chloride (3).
Benzamide (ane) was refluxed under aqueous acidic conditions for 1 hour to yield benzoic acid (2). Acid (2) was then refluxed with SOCltwo to yield benzoyl chloride (three).
Sometimes a scheme may exist used to illustrate a non-chemical process or how an musical instrument's components are connected. These could also be presented as figures, and there is no definitive rule that will tell y'all when to use a scheme and when to employ a figure. When in incertitude, think of the reader and use the method that conveys the nigh information in the most easily understood format
Figures
Figures fall into two broad categories; those that are pictorial representations of concepts that are presented in the text, and those which summarize data. Again, it is critical to your report that your figures are clear, concise and readable, and that they back up the arguments that you are making. Remember that you must refer to and discuss every figure in the text! If a effigy is not mentioned, yous don't need it!
Figures that are pictorial representations of concepts normally appear in the Introduction, but it is as well appropriate to include them in the Discussion. Use this type of figure to make your writing more than concise (think the conversion cistron: 1 picture = one kword). Recall, humans are very visually oriented and we tin grasp circuitous concepts presented as picture more hands then when they are presented in words or as mathematical formulae. Some examples of concept figures include:
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- 1) An illustration of the deposition of metals onto a silicon wafer.
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- 2) A diagram of the HIV life cycle.
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- 3) A depiction of microwaves exciting h2o molecules.
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- four) A diagram illustrating the Frank-Condon principle.
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- v) A proposed organic machinery.
Graphs are figures that present data. You apply a graph when you take more data than will fit in a table. The general rules for preparing good figures for your notebook likewise utilise in a laboratory study (click here to review graph preparation). Formatting tips: do non use colored backgrounds or gridlines, and practice not draw a box around the graph.
You may find information technology more than curtailed to combine all your data into one graph. For example, it may be advisable to put six lines with absorbance as a function of time, with varying concentrations of a reactant on the same graph rather than amalgam 6 dissimilar graphs. However, when doing this, be careful not to over-ataxia the graph.
Standard curves should not be included in this section unless that was the primary goal of the experiment. They should be put in the Supporting Information.
Figures have figure captions compiled in the Figure Legend department, located on a separate page at the stop of the newspaper. Journals chose this format because of typographical issues, and it has been retained despite its inconvenience to the reader. Each effigy should announced on its own folio in the lodge is it is discussed in the text. Effigy captions appear in the Figure Legends section and exercise not announced on the same page as the figure. Withal, in the bottom, right-paw corner of the page the post-obit identifying text appears:
- "First author's last name et al., Effigy number"
Figure Legends
All figure legends (captions) should exist found in the section entitled "Figure Legends". The format for a effigy legend is usually: "Figure number" (italics and bold), a short title (followed past a menstruation) and and so a description of what is in the figure. All figure legends are compiled on the aforementioned page separated past a blank line. Exist certain to define in the caption any symbols used in the effigy, and note whether lines that laissez passer through data points are fits, or "guides to the eye".
- Example Figure Explanation
- Figure 1. Nucleic acid bases. The chemical structures of (a) adenine, (b) guanine, (c) cytosine, and (d) thymine.
Supporting Data
This section (also known as Supplemental Material) is where you can include information that may be helpful, but not essential, for evaluation of your data. Items in this department may include calibration curves, and spectra (from which you extracted simply i absorbance value for your analysis). Figures or tables of data whose contents were summarized in the text, or which were not disquisitional to the conclusions, are also to be placed in the supporting information. An example of this type of material is the table of atom positions generated in an Ten-ray crystal structure.
References
- 1. Click here to obtain this file in PDF format. (link non yet active)
- 2. Click here for an example of a completed laboratory written report.
- three. The ACS Style Guide; 2nd ed.; Dodd, J. S., Ed.; American Chemical Society: Washington, D.C., 1997.
- 4. Booth, West. C.; Colomb; K. G.; Williams, J. One thousand. The Craft of Inquiry The University of Chicago Press: Chicago, IL, 1995.
- 5. Spector, T. J. Chem. Educ. 1994, 71, 47-50. Click here to view as a PDF file (Truman addresses only).
- 6a. Journal of the American Chemical Society Instructions for Authors, 2007.
- b. Inorganic Chemistry Teaching for Authors, 2007.
- c. Chemic Reviews Instructions for Authors, 2007.
- 7. Whatsoever non-English word should be italicized. This includes Greek and German language words, and their abbreviations, that appear as function of chemical names (e. one thousand., ortho-, meta-, para-, cis-, trans-, E-, Z-, alpha-, beta-, etc.). Besides italicized are the condensed forms of secondary (sec-), tertiary (tert-), etc. The main exception to the rule for italicizing non-English language words are the Greek and Latin prefixes that announce numbers in chemical names (eastward. g., mono-, bi-, tri-, etc.). Some common Latin phrases that appear in scientific writing are vide infra ("see later"),vide supra ("run across earlier"), et al. (abbreviation of et alia, Latin for "and others"), eastward. one thousand. (from Latin exempli gratia, "for example", not usually italicized) and i. due east. (from Latin id est, "it is", also not usually italicized). Other Latin phrases and abbreviations ordinarily used in footnotes and references (e. 1000., op. cit.) are not used in scientific writing.
How To Set Up A Science Lab Report,
Source: https://chemlab.truman.edu/the-laboratory-report/
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